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UNK36.TXT
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1993-02-13
|
4KB
|
207 lines
The unknown dissolved only in concentrated sulfuric acid.
1348
This indicates that the unknown is a neutral, oxygen-containing compound.
Signal near 2.1 ppm is exchangeable. Deuterochloroform solvent.
ΦσσσσσΣΣσσσµσσσσσσµσσσσΣσσΣΣΣΣΣΣσΣΣΣσσσσσµµµσσσσσσµτµσσσσσσσσσσΣΣσσσσσσσσσΣΣΣσσσσσΣσµµµΣΣσσΣΣΓΣσσσσσσσµσσµµµµσσΣσσσσµµσσσσσσΣσµµσσσσΣσσσµσµσσσσµτττµσσΣΣΣσσµµµσσσσσΣσσµµσσσσσσσΣΣσµµµµµµσσσΣΣΣΣΣΣσστµµµµµµµσσΣΣσµµµµµµµµµµµµτµΣστΣσσσµµµµµµµµτµσσσµτΦτµµµµµµτττ
τµµσµµτττµµτττµµµµµµΣσσσσσσσσµµµµµµττττττττµµµµµµσΣΣΣσσΣΣσσσσµµµµµµµτττµµµµµµµµµτµµσπß▌╓╬╧┌▌ßΓ▀╨╟╛┬╒▌α▄╥═╥▄αßαßΓΓΓΣµµττπσσΣττττµµττττττττττττµµτττµτττµτττσµΦτττµτττΦττττΣµµµµµµµττµσσΣσσσµµµµµσσσσσµµσπΓß█╘╠┐╗╡┐╚┌▌αππΣΣΣσµΣσσΣΣπππΣµµσπß▀▀Γα▌▄┌╪╙╨╘╒╒╘╘┬╗└╞╬╘
┘┌╪╙═╔╘█▌αßΓ▐ααßΓΣµσσΣΣΣΣπαµßß╪╧╧¢B *f»│âûhTi╜Ñ╝▐ΓµσττΦΦτττµµµµτττΦΦττµστττσΣΣΣµτττΣΣσµτΦΦΦΦΦΦττ█┘╠╬╪ΣµµµττΦΦΦττΦΦΦΦö╢"╣╢!╚╢#╓ &
#
The unknown is a saturated aliphatic alcohol with 12 ( or multiple ) H's.
#
dummy ms
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#
#
#
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No extra elements were detected.
212531353941424349264048
Elements like sulfur, nitrogen and the halogens are absent.
The compound burnt with a clear flame and left no residue.
#
The compound is saturated and not a metal salt.
Below room temperature.
#
A requirement for a liquid.
Liquid film
((((((((((('(((''''&&%%%&&'(),-.26=AKR]itêÅÿíº»╖╝└╟╩╠╬╨╥╘╫╪┘┌┌┌┌┘╪╫╓╒╙╨═╔┼└╣│«ºáûæïå{xusssÇå┐ΣΦΣ▀αα▌┌╫╘╪╒╟╣¼áöÄå{snljhgjfb[VTPONLIHGFEC@=;9764310///-,+*)))(''&%%%$$$###""""""!!!"!!"#$&&$$$#!! !!""#"""!!! !!!!!!!!!!!!!!"#$&''()++*)(''(
(((((())))))***,,,,,.//00124458:>@CGWiïù»╜║╡░ÜÄîÄÅèêåäàƪóÖ¥½ùçé~{xvrnie^[XUUY[[[[[Y[^adggd]OICABIQe_QLRXbo|üüvg_WMpq~ó╚╨╤╩╝┤£åï»╕½ÜêzoozÅÅm^O@F@:34;54;8,$!!"$',5Ee]G:45:?AABLTYZ[YWTUWZ_`bdfghjkmmmmmmmlljihgfea_]ZVSPKHEC@==>@=82/--,182+%"#&&$" "!%'&
141922242729423153
This compound is a saturated aliphatic alcohol.
129-132 degrees.
#
A typical value for a liquid.
Optically inactive.
#
The molecule is not chiral.
0.809
#
Typical for an organic liquid.
1.409
#
A typical value.
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dummy cmr
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No precipitate was formed.
2227282950
The compound is not a ketone or an aldehyde.
A vigorous reaction with gas evolution took place.
#
This reaction indicates an active H (e.g. alcohol, phenol or water if not dry).
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#
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No change was seen.
14
The unknown is not an ester.
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A rapid reaction occurred which gave a sweet-smelling liquid.
#
The unknown is an alcohol which reacted to form an ester (smell).
#
#
#
On standing for a long time at room temperature a reaction occurred.
#
The unknown is saturated but can be slowly oxidised (due to an alcohol group ?).
An aldehyde was obtained as the product.
#
Only a primary alcohol can be oxidised to an aldehyde.
No colour change was observed.
232850
The unknown is not a sugar.
#
#
#
No reaction was observed.
#
The unknown is is not unsaturated nor is it a phenol.
No positive result.
#
The compound is not an ether.
No reaction could be seen.
#
The unknown is not a phenol.
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No change could be seen.
#
This liquid is not a 1,2-diol.
No positive reaction.
#
The unknown is not a 1,2-diol.
A rapid reaction occurred.
#
The unknown is a primary or secondary alcohol.
Very vigorous reaction - a solution was obtained.
#
This is typical of an oxygen-containing compound.
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A clear solution was formed.
#
The unknown is a low molecular weight primary alcohol.
No change was noted.
#
The compound is not a phenol nor is it unsaturated.
No reaction took place.
#
The compound is not an ester, acetal, amide, nitrile etc.
A reaction occurred giving a liquid.
#
The compound is an alcohol (prim. or sec. amines would give solids).
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colourless liquid
010509
203054
74757684
Solid m.p. 66-69 degrees.
Colourless crystals m.p. 164-167 degrees.
Solid with melting range of 61 to 63 degrees.
Solid m.p. range 55-57 degrees.
3
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ƒ├╡▒¡┴lÇ│iç╣ñ░╜
ª┬»╜ì▒s»│j¥╢|ó╜╡l¡╕f
liquid aliphatic alcohol
4
2-methyl-3-pentanol
2-methyl-1-butanol
Isoamyl alcohol
3-hexanol